Vent-air purification system |
The vent air purification system allows hexane to be recovered in the solvent extraction plant instead of letting it escape to the atmosphere. This innovation results in a hexane loss of below 1 kg per metric ton of feed material processed, which is an achievement unparalleled by other method.
Process description
To create vacuum in the toaster, conveying equipment, extractor and other equipment except in the distillation section, we use ejector or fans at the final vent at a pressure of about 0.5 kg per cm2. By adopting the new system this pressure can be increased upto 7 kg per cm2 without any additional loss to the atmosphere. As a result all the equipment will be under an adequate vacuum because desolventisation efficiency can be improved. Thus, solvent losses will be at the minimum. We have observed that during continuous operation out of the total hexane losses 35% are through vent air, 40% through desolventising toaster, 5% through oil, and 20% through leakages. By adopting the new system all these losses except through oil can be reduced by upto 90%.
In our new system, the vent air is taken back into the vent air purification system instead of discharging to atmosphere, where the air is dissolved in the water by high pressure mixing method. Hexane is arrested by water, which is then taken into the water separator and hexane is recovered for re-use. The final traces of hexane and air that escape from the purification system are taken to the extractor where the hexane is absorbed by the raw material and the air is discharged.
With the adoption of the vent air purification system, there is no need of a refrigeration unit in the project to condense the hexane.
Mecpro offers
| • Hexane loss below 1 kg/ton from the Indian average of 11 kg/ton |
| • Pollution is greatly reduced |
| • No refrigeration unit required |
| • Offset the operators' mistakes |
| • Minimum hexane loss in the desolventizing and startup stages |
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Low temperature miscella separation (Patented) |
This is a process of separating hexane from the miscella at a low temperature. It is achieved by means of azeotropic distillation using a reflux column. A reflux column is designed to perform the most efficient distillation of hexane from the miscella so that the maximum possible amount of hexane is recovered at a lower temperature. The process has been perfected in a series of laboratory trials and actual implementation in India and abroad.
Process description
After conducting a detailed study of the conventional process of hexane separation and the excessive losses of hexane, deterioration of oil and development of non-hydratable phosphatides therein, we have developed a new process named azeotropic distillation. It refers to a process in which a component (known as the solvent or entrainer) is added at the top of the column to form a homogeneous complex known as an azeotrope, which is removed as distillate itself. The other component free from the solvent is collected at the bottom of the column. In this case, the process is quite different from the normal stripping distillation because the solvent that appears as distillate can be separated at a lower temperature and refluxed at the top of the column for augmentation of the process.
In isothermal distillation, no physical or chemical changes take place to any of the components present. The complex formed in the vapour filter is fed to the reflux column where the hexane separation takes place isothermally at 65oC, the vapourising temperature of hexane.
By means of the reflux column, miscella separation at 65o C for non-frothing oil and 75oC to 85oC in frothing oil like soybean and mustard is achieved. Plants not using the reflux column separate the miscella at an elevated temperature of 120oC with sparged steam, due to which oxidation of oil and degradation occur. Also steam sparged at this elevated temperature in the stripper increases non-hydratable phosphatides which increases the refining loss. At a lower temperature with a reflex column water degumming is possible provided harvesting and storage of the seed was proper.
Mecpro offers
| • Reduced steam consumption |
| • Reduced chemical consumption in refining process |
| • Better oil colour |
| • Higher bleach ability |
| • Less increase in FFA as compared to any other method |
| • Less non-hydratable phosphatides development than any other method |
| • Less peroxide value than any other method |
| • Less anisidine value than any other method |
| • No oxidisation or degradation of oil |
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